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Step 5: Draw the Bacteriostatic Water Using a sterile syringe with an appropriate needle, draw the calculated volume of bacteriostatic water from the BAC water vial
Then 3,4-dimethoxyphenethylamine was added (1.25 mmol) and the solution cooled to 0C before dichloromethane solution containing 4-DMAP (40 mg) was added dropwise to the reaction system, which was maintained at 0C for 1 hour