Potassium Phosphate Tribasic FCC Hypnotic APIs 10% BARIUM TO PASS TEST

10% BARIUM TO PASS TEST TO PASS TEST RESIDUAL SOLVENTS TO PASS TEST TO PASS TEST MICROBIAL LIMITS TOTAL AEROBIC MICROBIAL COUNT 100 CFU/g TOTAL YEAST AND MOLD COUNT 100 CFU/g ESCHERICHIA COLI Negative Negative SALMONELLA Negative Negative STAPHYLOCOCCUS AUREUS Negative Negative PSEUDOMONAS AERUGINOSA Negative Negative

00% HEAVY METALS (as Pb) 5 ppm HEAVY METALS (as Pb) 5 ppm IRON (Fe) 5 ppm IRON (Fe) 5 ppm IDENTIFICATION TO PASS TEST TO PASS TEST IDENTIFICATION TO PASS TEST TO PASS TEST

Test Specification Min Max DNase NONE DETECTED NONE DETECTED ENDONUCLASE NONE DETECTED NONE DETECTED RETEST DATE

01% GLUCOSE 0

0 % pH OF A 0

Potassium Phosphate Tribasic FCC Hypnotic APIs 10% BARIUM TO PASS TESTTest Specification Min Max ASSAY (IGNITED) 97. 00% 97. 00% ARSENIC (As) 3 mg kg FLUORIDE 10 mg kg INSOLUBLE SUBSTANCES 0. 20% LEAD (Pb) 2 mg kg LOSS ON IGNITION 5. 00% IDENTIFICATION TO PASS TEST TO PASS TEST RETEST DATE